반응 #471780

반응 방정식

3-Aminopropyltriethoxysilane

6-(4-methoxy-benzoyl)-7-oxa-bicyclo[4.2.0]octan-8-one

→

title compound

2-Hydroxy-2-(4-methoxybenzoyl)cyclohexanecarboxylic acid(3-silanyl-propyl)-amide

용매

methylene chloride

반응 조건

후처리

1. 1
   온도The reaction mixture is heated
2. 2
   온도at reflux for several hours
3. 3
   기타Upon completion of the reaction, solvent
4. 4
   기타is evaporated

실험 절차

3-Aminopropyltriethoxysilane (22.14 g, 0.100 mol) is added to a solution of 26.03 g (0.100 mol) of 6-(4-methoxy-benzoyl)-7-oxa-bicyclo[4.2.0]octan-8-one in methylene chloride. The reaction mixture is heated at reflux for several hours and monitored by thin layer chromatography. Upon completion of the reaction, solvent is evaporated to obtain the title compound.

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