반응 #47168
ord-c283994b4e15486abaa57cea0e2ef7d8
반응 방정식
(2-Amino-5-bromo-phenyl)phenyl-methanone
4-Methoxy-benzenesulfonyl chloride
→
title compound
N-(2-Benzoyl-4-bromo-phenyl)-4-methoxy-benzenesulfonamide
반응물
시약
없음
반응 조건
상세 조건
See reaction.notes.procedure_details.
실험 절차
The title compound was prepared according to the general procedure for the synthesis of N-Aryl-benzenesulfonamides previously described using 138 mg of (2-Amino-5-bromo-phenyl)phenyl-methanone and 103 mg of 4-Methoxy-benzenesulfonyl chloride. 1H-NMR (400 MHz, CDCl3): δ 3.78 (s, 3H), 6.83 (d, 2H, J=9.2 Hz), 7.39 (b, 1H), 7.49 (d, 2H, J=6.4 Hz), 7.68 (m, 4H), 8.85 (d, 2H, J=6.0 Hz), 9.96 (b, 1H). MS: m/z 447.0 (M++1).