반응 #470371

반응 방정식

N-methoxymethyl-N-methylpyrrolidinium chloride

N-Methoxymethyl-N-Methylpyrrolidinium Chloride

potassium hexafluorophosphate

→

white solid

N-Methoxymethyl-N-Methylpyrrolidinium hexafluorophosphate

용매

water

반응 조건

후처리

1. 1
   기타separated out
2. 2
   workup.ADDITIONdichloromethane was thereafter added to the mixture for extraction
3. 3
   세척The organic layer was washed with 120 g of water six times
4. 4
   기타dried

실험 절차

A 20.0 g quantity of N-methoxymethyl-N-methylpyrrolidinium chloride prepared in Example 10 was dissolved in 120 g of water, and 22.2 g of potassium hexafluorophosphate was added to the solution, whereupon a white solid separated out. The mixture was stirred for 30 minutes, and dichloromethane was thereafter added to the mixture for extraction. The organic layer was washed with 120 g of water six times and then dried, affording 25.1 g of a white solid as the desired product.

출처