반응 #470369

반응 방정식

trifluoromethanesulfonic acid

N-methoxymethyl-N-methylpyrrolidinium chloride

N-Methoxymethyl-N-Methylpyrrolidinium Chloride

→

trifluoromethanesulfonic acid

desired product

N-Methoxymethyl-N-Methylpyrrolidinium

용매

methanol

methanol

MeOH

반응 조건

후처리

1. 1
   기타to remove hydrogen chloride
2. 2
   기타produced as a by-product

실험 절차

A 30.0 g quantity of N-methoxymethyl-N-methylpyrrolidinium chloride prepared in Example 10 was dissolved in 30.0 g of MeOH, and 80.0 g of methanol solution of 35 wt. % trifluoromethanesulfonic acid was added to the solution. The mixture was heated at 130° C. in a nitrogen stream to remove hydrogen chloride produced as a by-product, an excess of trifluoromethanesulfonic acid and methanol, giving 49.0 g of the desired product.

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