반응 #470367

반응 방정식

Methoxymethylpyrrolidine

dimethyl carbonate

→

desired product

수율 60.0%

N-Methoxymethyl-N-Methylpyrrolidinium Methyl carbonate

수율 60.0%

반응 조건

후처리

1. 1
   기타reacted at 120° C. for 24 hours
2. 2
   여과The resulting solids were filtered off
3. 3
   세척washed with dimethyl carbonate
4. 4
   기타The solids were dried in a vacuum

실험 절차

Methoxymethylpyrrolidine (10.00 g) and 117.39 g of dimethyl carbonate were placed into an autoclave and reacted at 120° C. for 24 hours. The resulting solids were filtered off and washed with dimethyl carbonate. The solids were dried in a vacuum, giving 10.70 g of the desired product.

출처