반응 #465935

ord-02c47444813f491eb7b99c1d7a363f28

반응 방정식

COc1ccccc1OC
1,2-dimethoxy benzene
O=C(Cl)c1ccccc1
benzoyl chloride
[Al+3].[Cl-].[Cl-].[Cl-]
aluminum chloride
COc1ccc(C(=O)c2ccccc2)cc1OC
3,4-dimethoxy benzophenone
수율 95.7%

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

The process of Step 1, Example 4 was followed except that 292 grams of 1,2-dimethoxy benzene, 297 grams of benzoyl chloride, and 281 grams of aluminum chloride were used to yield 490 grams of 3,4-dimethoxy benzophenone.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US06296785B1uspto-grants-2001_10