반응 #465571

반응 방정식

N-phenyl-o-phenylenediamine

3,4,5-trimethoxybenzoyl chloride

→

N-[(3,4,5-trimethoxyphenyl)carbonyl]-N'-phenyl-phenylenediamine

용매

diethyl ether

diethyl ether

반응 조건

후처리

1. 1
   workup.ADDITIONwas added dropwise
2. 2
   기타The solvents were then removed in vacuo

실험 절차

A solution of N-phenyl-o-phenylenediamine (1.84 g, 10 mmol) in diethyl ether (90 ml) was stirred at room temperature as 3,4,5-trimethoxybenzoyl chloride (2.31 g, 10 mmol) in diethyl ether (40 ml) was added dropwise. The reaction mixture was then stirred overnight at room temperature. The solvents were then removed in vacuo leaving N-[(3,4,5-trimethoxyphenyl)carbonyl]-N'-phenyl-phenylenediamine.

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