반응 #4629
ord-a1f901233c8e48c982691f27cf0723c8
반응 방정식
5-(2-bromoethoxy)salicylamide
1-(2-allyloxyphenoxy)-3-aminopropan-2-ol
→
1-(2-allyloxyphenoxy)-3-[2-(3-carbamoyl-4-hydroxyphenoxy)ethylamino]propan-2-ol
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타is melted in an oil bath at 100°
실험 절차
A mixture of 6.5 g of 5-(2-bromoethoxy)salicylamide and 8.9 g of 1-(2-allyloxyphenoxy)-3-aminopropan-2-ol is melted in an oil bath at 100° and stirred for 1 hour using a magnetic stirrer. The working up is carried out analogously to Example 11 and yields 1-(2-allyloxyphenoxy)-3-[2-(3-carbamoyl-4-hydroxyphenoxy)ethylamino]propan-2-ol having a melting point of 147°-148° (from isopropanol).