반응 #462499

반응 방정식

5,6-diamino-1,3-dipropyluracil

2,4 -dimethoxy-3-methylcinnamic acid

→

Compound 14

수율 50.1%

(E)-8-(2,4-Dimethoxy-3-methylstyryl)-1,3-dipropylxanthine

수율 50.1%

반응 조건

후처리

1. 1
   기타Then, the resultant crude crystals were recrystallized from dioxane/water

실험 절차

Substantially the same procedure as in Reference Example 1 was repeated using 1.25 g (5.52 mmol) of 5,6-diamino-1,3-dipropyluracil and 1.35 g (6.08 mmol) of 2,4 -dimethoxy-3-methylcinnamic acid. Then, the resultant crude crystals were recrystallized from dioxane/water to give 1.14 g (yield 50%) of Compound 14 as white needles.

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