반응 #462498

반응 방정식

5,6-diamino-1,3-dipropyluracil

4-methoxy-2,3-dimethylcinnamic acid

→

Compound 12

수율 48.3%

(E)-8-(4-Methoxy-2,3-dimethylstyryl)-1,3-dipropylxanthine

수율 48.3%

반응 조건

후처리

1. 1
   기타Then, the resultant crude crystals were recrystallized from dioxane/water

실험 절차

Substantially the same procedure as in Reference Example 1 was repeated using 2.31 g (10.24 mmol) of 5,6-diamino-1,3-dipropyluracil and 2.42 g (15.4 mmol) of 4-methoxy-2,3-dimethylcinnamic acid. Then, the resultant crude crystals were recrystallized from dioxane/water to give 1.96 g (yield 48%) of Compound 12 as a white powder.

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