반응 #462473

반응 방정식

5,6-diamino-1,3-dipropyluracil

3- (4-methoxynaphthyl)acrylic acid

→

Compound 61

수율 56.1%

(E)-8-[2-(4 -Methoxynaphthyl)vinyl]-1,3-dipropylxanthine

수율 56.1%

반응 조건

후처리

1. 1
   기타Then, the resultant crude crystals were recrystallized from dioxane/water

실험 절차

Substantially the same procedure as in Reference Example 1 was repeated using 3.0 g (13.3 mmol) of 5,6-diamino-1,3-dipropyluracil and 3.33 g (14.6 mmol) of 3- (4-methoxynaphthyl)acrylic acid. Then, the resultant crude crystals were recrystallized from dioxane/water to give 3.12 g (yield 56%) of Compound 61 as yellow needles.

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