반응 #452417

반응 방정식

3-(n-heptylamino)phenol

2-bromoethanol

NaHCO3

→

3-[N- (n-heptyl)-N-(2-hydroxyethyl) -amino]phenol

수율 54.0%

용매

methanol

반응 조건

후처리

1. 1
   온도After cooling
2. 2
   여과the mixture is filtered
3. 3
   기타the solvent is removed in vacuo

실험 절차

0.1 mol of 3-(n-heptylamino)phenol in 100 ml of methanol is refluxed for 10 h with 0.11 mol of 2-bromoethanol and 0.1 mol of NaHCO3. After cooling, the mixture is filtered, the solvent is removed in vacuo, and the residue is fractionated, to give 3-[N- (n-heptyl)-N-(2-hydroxyethyl) -amino]phenol.

출처