반응 #452414

반응 방정식

n-butyl bromide

NaHCO3

m-aminophenol

→

3-(n-butylamino)phenol

수율 57.0%

용매

methanol

반응 조건

후처리

1. 1
   온도the mixture is refluxed for 5 h
2. 2
   온도After cooling
3. 3
   여과it is filtered
4. 4
   기타the solvent is removed in vacuo

실험 절차

0.11 mol of n-butyl bromide and 0.1 mol NaHCO3 are added to 0.1 mol of m-aminophenol in 150 ml of methanol, and the mixture is refluxed for 5 h. After cooling, it is filtered and the solvent is removed in vacuo. The oil which remains is fractionated in vacuo, to give 3-(n-butylamino)phenol.

출처