반응 #451340
ord-fa4cadfbf86f465b86bc3bbc95423f31
반응 방정식
N-vinylpyrrolidone
tert-butyl methacrylate
polypropylene
azobisisobutyronitrile
→
allyl methacrylate
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1workup.ADDITIONwas added to the mixture
실험 절차
The dimer of allyl methacrylate, which was prepared according to Example 1, was added to the mixture containing 97 wt.-% N-vinylpyrrolidone and 3 wt.-% tert-butyl methacrylate in the amount of 1 wt. % on the whole mixture. The mixture was polymerized in a polypropylene mold at 60° C. for 16 h in the presence of 0.4 wt.-% azobisisobutyronitrile. The resulting gel contained, after swelling with water, 90 wt.-% water at G=0.038 MPa.