반응 #451338
ord-0c898061a2e84a4b86bc75b954ef6864
반응 방정식
N-vinylpyrrolidone
dodecyl methacrylate
polypropylene
azobisisobutyronitrile
→
allyl methacrylate
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1workup.ADDITIONwas added in the amount of 3 wt.-% (
실험 절차
The dimer of allyl methacrylate, which was prepared according to Example 1, was added in the amount of 3 wt.-% (based on to the entire mixture) to the mixture containing 90 wt.-% N-vinylpyrrolidone and 10 wt.-% dodecyl methacrylate. The mixture was polymerized in a polypropylene mold at 60° C. for 16 h in the presence of 0.4 wt.-% azobisisobutyronitrile. The resulting gel contained, after swelling with water, 76 wt.-% water at G=0.048 MPa. The soluble extractable portion was 2%.