반응 #451338

ord-0c898061a2e84a4b86bc75b954ef6864

반응 방정식

C=CN1CCCC1=O
N-vinylpyrrolidone
C=C(C)C(=O)OCCCCCCCCCCCC
dodecyl methacrylate
CC(C[*:1])[*:2]
polypropylene
CC(C)(C#N)N=NC(C)(C)C#N
azobisisobutyronitrile
C=CCOC(=O)C(=C)C
allyl methacrylate

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    workup.ADDITIONwas added in the amount of 3 wt.-% (

실험 절차

The dimer of allyl methacrylate, which was prepared according to Example 1, was added in the amount of 3 wt.-% (based on to the entire mixture) to the mixture containing 90 wt.-% N-vinylpyrrolidone and 10 wt.-% dodecyl methacrylate. The mixture was polymerized in a polypropylene mold at 60° C. for 16 h in the presence of 0.4 wt.-% azobisisobutyronitrile. The resulting gel contained, after swelling with water, 76 wt.-% water at G=0.048 MPa. The soluble extractable portion was 2%.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04604440uspto-grants-1986_08