반응 #451337

ord-637b6b28676a407aa2efc9ed4d504916

반응 방정식

CC(C)(C#N)N=NC(C)(C)C#N
azobisisobutyronitrile
CC(C[*:1])[*:2]
polypropylene
C=CN1CCCC1=O
N-vinylpyrrolidone
C=C(C)C(=O)OCCCCCCCCCCCC
dodecyl methacrylate
O=O
oxygen
C=CCOC(=O)C(=C)C
allyl methacrylate

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    workup.ADDITIONwas added in the amount of 1 wt.-% (

실험 절차

The dimer of allyl methacrylate, which was prepared accordin9 to Example 1, was added in the amount of 1 wt.-% (related to the entire mixture) to the mixture containing 70 wt.-% N-vinylpyrrolidone and 30 wt.-% dodecyl methacrylate. The mixture was homogenized, freed of air oxygen and polymerized in the presence of 0.4 wt.-% azobisisobutyronitrile in a polypropylene mold at 60° C. for 16 h. The resulting gel contained, after swelling with water, 77 wt.-% water at G=0.067 MPa.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04604440uspto-grants-1986_08