반응 #451337
ord-637b6b28676a407aa2efc9ed4d504916
반응 방정식
azobisisobutyronitrile
polypropylene
N-vinylpyrrolidone
dodecyl methacrylate
oxygen
→
allyl methacrylate
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1workup.ADDITIONwas added in the amount of 1 wt.-% (
실험 절차
The dimer of allyl methacrylate, which was prepared accordin9 to Example 1, was added in the amount of 1 wt.-% (related to the entire mixture) to the mixture containing 70 wt.-% N-vinylpyrrolidone and 30 wt.-% dodecyl methacrylate. The mixture was homogenized, freed of air oxygen and polymerized in the presence of 0.4 wt.-% azobisisobutyronitrile in a polypropylene mold at 60° C. for 16 h. The resulting gel contained, after swelling with water, 77 wt.-% water at G=0.067 MPa.