반응 #44956
ord-60044640ac4f49cfa96a7c565ef0c340
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1여과The solution was filtered
- 2기타the methanol was evaporated from the filtrate at reduced pressure
- 3기타to give a final volume of 30 ml
- 4기타dried
실험 절차
Pseudomonic acid (10.01 g, 20 mmole) was dissolved in a mixture of methanol/water (50 ml and 36 ml). Calcium oxide (0.78 g, 14 mmole) was added portionwise to the mixture and was stirred for 1 h. The solution was filtered, and the methanol was evaporated from the filtrate at reduced pressure to give a final volume of 30 ml. Water (20 ml) was added to the solution. Then the solution was freeze dried to obtain 9.11 grams of product.