반응 #44825

반응 방정식

2-chlorobenzimidazole

2-aminoindane

→

title compound

N-(Benzimidazol-2-yl)-2-indanylamine

반응 조건

후처리

1. 1
   기타The product was isolated by preparative LCMS

실험 절차

The title compound was prepared from 2-chlorobenzimidazole and 2-aminoindane by Procedure A (15 min at 150° C.). The product was isolated by preparative LCMS to give the title compound as the free base (white solid, mp 246-249° C.). MS(ES+) m/z 250 ([M+1]+, 100). 1NMR (DMSO-d6) δ 2.91 (dd, 2H), 3.29 (dd, 2H), 4.35 (m, 1H), 6.80-6.92 (m, 3H), 7.10-7.17 (m, 4H), 7.22-7.25 (m, 2H), 10.60 (s, 1H).

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