반응 #446099

반응 방정식

1-Naphthalenemethanol

1,5-dibromopentane

→

title compound

1-[[(5-Bromopentyl)oxy]methyl]naphthalene

반응 조건

후처리

1. 1
   세척FCC eluting with ether-cyclohexane (1:49→2:48)

실험 절차

1-Naphthalenemethanol (6.00 g) and 1,5-dibromopentane (11.5 ml) were treated according to the method of Intermediate 1. FCC eluting with ether-cyclohexane (1:49→2:48) gave the title compound as a colourless oil (8.41 g), t.l.c. (Cyclohexane-ether 19:1) Rf 0.22;

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