반응 #442308

ord-09fb26f93d8c461e85c8867a503f8e60

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타Recrystallization from ether-hexane
  2. 2
    기타yields the product, m.p. 177°-178° C.

실험 절차

2-Bromo-5-chlorosulfonylbenzoic acid is reacted with 3-benzyloxypiperidine by the method of Example 1. Recrystallization from ether-hexane, yields the product, m.p. 177°-178° C.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04377521uspto-grants-1983_03