반응 #442307

반응 방정식

1-Acetyl-3-benzyloxypiperidine

sodium hydroxide

potassium carbonate

→

3-Benzyloxypiperidine

용매

water

반응 조건

후처리

1. 1
   온도refluxed for 24 hours
2. 2
   추출extracted three times with ether
3. 3
   기타The ether is removed by evaporation
4. 4
   workup.DISTILLATIONthe yellow oil is distilled at 92°-94° C. (0.3 mm Hg.)

실험 절차

1-Acetyl-3-benzyloxypiperidine (0.043 mole), sodium hydroxide (0.086 mole) and water (30 ml.) are combined and refluxed for 24 hours. The reaction mixture is saturated with potassium carbonate and extracted three times with ether. The ether is removed by evaporation and the yellow oil is distilled at 92°-94° C. (0.3 mm Hg.).

출처