반응 #4407

반응 방정식

2-(4-ethylthio-3-methylpyrid-2-yl)-thiazolo[3,2-a]benzimidazole

m-chloroperoxybenzoic acid

→

title compound

2-(4-Ethylthio-3-methylpyrid-2-yl)thiazolo[3,2-a]benzimidazole-1-oxide

용매

CH2Cl2

반응 조건

후처리

1. 1
   세척The solution is then washed with sodium carbonate solution
2. 2
   건조dried (MgSO4)
3. 3
   기타Purification by chromatography on silica

실험 절차

A solution of 2-(4-ethylthio-3-methylpyrid-2-yl)-thiazolo[3,2-a]benzimidazole (0.01 mole) is dissolved in CH2Cl2 solution (100 ml) at 0° C. and treated with m-chloroperoxybenzoic acid (0.01 mole) for 0.5 hours. The solution is then washed with sodium carbonate solution and dried (MgSO4). Purification by chromatography on silica gives the title compound.

출처