반응 #43719

반응 방정식

(2-chloro-3-nitrophenyl)methanol

→

2-Chloro-3-nitrobenzaldehyde

용매

chloroform

반응 조건

후처리

1. 1
   온도under reflux for 20 h
2. 2
   여과The mixture is filtered through kieselguhr
3. 3
   농축concentrated
4. 4
   기타dried under high vacuum
5. 5
   기타The resulting title compound is directly reacted further

실험 절차

9.2 g (49.05 mmol) of (2-chloro-3-nitrophenyl)methanol and 13.2 g (151.8 mmol) of activated manganese(IV) oxide in 50 ml of chloroform are heated under reflux for 20 h. The mixture is filtered through kieselguhr, concentrated and dried under high vacuum. The resulting title compound is directly reacted further.

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