반응 #433015
ord-11f7e682a4f24084bbe9185d193be591
반응 방정식
반응 조건
상세 조건
See reaction.notes.procedure_details.
실험 절차
7-Benzyl-2,7-diazabicyclo[3.3.0]octane (Example Jc) is reacted with ethyl chloroformate analogously to Example Oa) to give ethyl 7-benzyl-2,7-diazabicyclo[3.3.0]octane-2-carboxylate, and this is then debenzylated hydrogenolytically analogously to Example Jd). A colorless oil of boiling point 90° C./0.1 mbar is obtained.