반응 #432376

반응 방정식

2-Methylbenzothiazole

ethyl p-toluenesulfonate

→

3-ethyl-2-methyl-benzothiazolium p-toluenesulfonate

용매

acetone

반응 조건

후처리

1. 1
   기타the temperature rising to about 200° C. due to the exothermic reaction
2. 2
   기타the product that precipitates
3. 3
   기타is removed by filtration with suction
4. 4
   세척washed with acetone
5. 5
   건조dried over phosphorous pentoxide

실험 절차

2-Methylbenzothiazole (300 pbw) and ethyl p-toluenesulfonate (440 pbw) are heated with stirring to 150° C., the temperature rising to about 200° C. due to the exothermic reaction. After 10 minutes, the mixture is poured into 2000 pbw of acetone, and the product that precipitates is removed by filtration with suction, washed with acetone and dried over phosphorous pentoxide.

출처