반응 #426678

반응 방정식

2-(2-methoxy-4-nitrophenyl)benzothiazole

Hexane THF

tin (II) dichloride dihydrate

→

title compound

수율 96.0%

2-(4-Amino-2-methoxyphenyl)benzothiazole

수율 96.0%

용매

EtOH

반응 조건

후처리

1. 1
   기타Prepared

실험 절차

Prepared as described in the Nitro Reduction section using 2-(2-methoxy-4-nitrophenyl)benzothiazole (0.1 g, 0.35 mmol) and tin (II) dichloride dihydrate (0.63 g, 2.8 mmol) in EtOH (12 ml) to give the title compound (0.086 g, 96%) as a pale orange solid after work-up and flash chromatography (2:1 Hexane/THF).

출처