반응 #42355
ord-92306b3288f94584930245ab3ab8e0d5
반응 방정식
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1농축The solution is concentrated under reduced pressure
실험 절차
To O-benzyl-N-(tert-butoxycarbonyl)homoserine (5.8 g, 18.9 mmol) in 20% methanol/benzene (72 mL) is added 2M trimethylsilyldiazomethane in hexane (12.3 mL, 24.5 mmol), and the reaction stirred at room temperature 1.5 h. The solution is concentrated under reduced pressure to give the title compound in pure form. ESI MS m/z 324.2 [M+H]+.