반응 #42335
ord-da90b0ae5963488daffc62f844ba69b8
반응 방정식
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타A 250 ml round bottom flask equipped with magnetic stir bar
- 2온도reflux condenser, and N2 inlet
- 3온도The solution was refluxed for 4 hours
- 4농축then concentrated in vacuo
- 5기타vacuum dried overnight
실험 절차
A 250 ml round bottom flask equipped with magnetic stir bar, reflux condenser, and N2 inlet was charged with 9.2 g methyl N-acetyl-3-[(1-propylbutyl)sulfonyl]alaninate in 50 ml acetic acid and 50 ml conc. HCl. The solution was refluxed for 4 hours then concentrated in vacuo. The residue was chased with toluene (2×) then vacuum dried overnight to yield 7.8 g of the desired 3-[(1-propylbutyl)sulfonyl]alanine HCl salt.