반응 #42146

ord-0b6a244a31ae4bdea68240493807b244

반응 방정식

CCCCP(CCCC)CCCC
Tri-n-butylphosphine
Cl
hydrochloric acid
[Na+].c1ccc([B-](c2ccccc2)(c2ccccc2)c2ccccc2)cc1
sodium tetraphenylborate
→
CCCC[PH+](CCCC)CCCC.c1ccc([B-](c2ccccc2)(c2ccccc2)c2ccccc2)cc1
tri-n-butylphosphonium tetraphenylborate
수율 53.0%

반응물

CCCCP(CCCC)CCCC
Tri-n-butylphosphine
Cl
hydrochloric acid
[Na+].c1ccc([B-](c2ccccc2)(c2ccccc2)c2ccccc2)cc1
sodium tetraphenylborate

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

Tri-n-butylphosphine is reacted with hydrochloric acid in the presence of sodium tetraphenylborate to produce tri-n-butylphosphonium tetraphenylborate (53% yield) (see Nonpatent Document 6).

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07728176B2uspto-grants-2010_06