반응 #42144
ord-26bcb57d0e5a476a8aaa17b3207a4354
반응 방정식
sodium tetraphenylborate
Tricyclohexylphosphine
fluoroboric acid
tricyclohexylphosphonium tetrafluoroborate
→
tricyclohexylphosphonium tetraphenylborate
수율 75.0%
반응물
시약
없음
반응 조건
상세 조건
See reaction.notes.procedure_details.
실험 절차
Tricyclohexylphosphine is reacted with fluoroboric acid to synthesize tricyclohexylphosphonium tetrafluoroborate, which is reacted with sodium tetraphenylborate to produce tricyclohexylphosphonium tetraphenylborate (75% yield). A similar process is described in which tri-tert-butylphosphine is used as starting material to produce tri-tert-butylphosphonium tetraphenylborate (71% yield) (see Nonpatent Document 4).