반응 #42045

반응 방정식

1-(2-methyl-5-nitrophenyl)guanidine nitrate

sodium hydroxide

→

objective compound

수율 100.1%

1-(2-methyl-5-nitrophenyl)guanidine

수율 100.1%

용매

반응 조건

후처리

1. 1
   여과The crystals were filtered
2. 2
   세척sufficiently washed with water
3. 3
   기타forced-air dried at 60° C.

실험 절차

To 135 g of 1-(2-methyl-5-nitrophenyl)guanidine nitrate (Japanese Unexamined Patent Publication (Kokai) No. 6-87834), 21 g of sodium hydroxide in 1.0 L of a cold aqueous solution was directly added, followed by stirring at room temperature for 10 minutes. The crystals were filtered, sufficiently washed with water and then forced-air dried at 60° C. to obtain 102 g of the objective compound as pale yellow crystals.

출처