반응 #420300

ord-b8ff775a343442dea1083eb2ec6797fd

반응 방정식

NS(=O)(=O)c1ccc(N=C=S)cc1
4-isothiocyanatobenzenesulfonamide
Nc1ccccc1I
2-iodoaniline
NS(=O)(=O)c1ccc(NC(=S)Nc2ccccc2I)cc1
4-(3-(2-iodophenyl)thioureido)benzenesulfonamide

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타The subject compound was prepared

실험 절차

The subject compound was prepared utilizing the procedure described above from 4-isothiocyanatobenzenesulfonamide and 2-iodoaniline. 1H NMR (400 MHz, DMSO-d6) δ 10.16 (s, 1H), 9.60 (s, 1H), 7.90-7.81 (m, 8H), 7.76 (bs, 2H); (M+H)+ (434).

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US08877970B2uspto-grants-2014_11