반응 #42009

반응 방정식

oleic acid

ethanol

→

ethyl oleate

수율 90.0%

용매

ether

반응 조건

후처리

1. 1
   온도was refluxed
2. 2
   workup.ADDITIONwas added
3. 3
   여과the catalyst was filtered off
4. 4
   농축concentrated

실험 절차

A mixture containing Catalyst A (0.05 g) and oleic acid (1.41 g, 5 mmol) and ethanol (10 ml) was refluxed with stirring for 40 h. On cooling ether (30 ml) was added and the catalyst was filtered off. The organic washings were combined and concentrated to give ethyl oleate as an oil (1.39 g, 90% yield).

출처