반응 #419786

반응 방정식

5-(2-tert-Butoxycarbonylethenyl)furan-2-carboxylic acid benzyl ester

→

title compound

수율 98.1%

5-(2-tert-butoxycarbonylethyl)-furan-2-carboxylic acid

수율 98.1%

용매

methanol

반응 조건

후처리

1. 1
   기타was removed by celite filtration
2. 2
   기타the solvent was evaporated under reduced pressure

실험 절차

5-(2-tert-Butoxycarbonylethenyl)furan-2-carboxylic acid benzyl ester (0.97 g, 2.80 mmol) was dissolved in methanol (50 mL), 10% palladium/carbon (0.1 g) was added, and the mixture was stirred at room temperature for 2 hours under a hydrogen atmosphere. After completion of the reaction, palladium/carbon was removed by celite filtration, and the solvent was evaporated under reduced pressure to give the title compound (0.66 g).

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