반응 #417934

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phenol

3-o-tolylpropanoyl chloride

→

product

수율 93.0%

Phenyl 3-(o-tolyl)propanoate

수율 93.0%

반응 조건

후처리

1. 1
   workup.DISTILLATIONdistilled at 127-129° C./0.05 mbar

실험 절차

The procedure as described in Example 4a) was repeated with phenol (48 mmol) and 3-o-tolylpropanoyl chloride (55 mmol). The crude product (12.4 g, 97%) was short path distilled at 127-129° C./0.05 mbar to yield 10.6 g (93%) of product as a colourless, semicrystalline oil.

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