반응 #417926

반응 방정식

sodium hydroxide

33

methyl 4-(undec-4Z-enyloxy)benzoate

→

white solid

수율 98.1%

4-(undec-4Z-enyloxy)benzoic acid

수율 98.1%

용매

methanol

반응 조건

후처리

1. 1
   온도The solution is refluxed for 20 hours
2. 2
   기타After evaporating off the solvent
3. 3
   추출extracted with DCM

실험 절차

550 μL of 1 N sodium hydroxide solution (550 μmol) are added portionwise to 109 mg of 33 (358 μmol) in methanol (4 mL). The solution is refluxed for 20 hours. After evaporating off the solvent, the reaction medium is acidified with 0.5 N HCl and extracted with DCM. 102 mg of a white solid are obtained, i.e. a yield of 98%.

출처