반응 #417924

반응 방정식

sodium hydroxide

29

methyl 2-(undec-4Z-enyloxy)benzoate

→

yellow oil

수율 99.5%

2-(undec-4Z-enyloxy)benzoic acid

수율 99.5%

용매

methanol

반응 조건

후처리

1. 1
   온도The solution is refluxed for 24 hours
2. 2
   기타After evaporating off the solvent
3. 3
   추출extracted with DCM

실험 절차

500 μL of 1 N sodium hydroxide solution (500 μmol) are added portionwise to 80 mg of 29 (263 μmol) in methanol (3 mL). The solution is refluxed for 24 hours. After evaporating off the solvent, the reaction medium is acidified with 0.5 N HCl and extracted with DCM. 76 mg of a yellow oil are obtained, i.e. a yield of 99%.

출처