반응 #417921

반응 방정식

acid 22

3-(undecyloxy)benzoic acid

oxalyl chloride

toluene

→

yellow oil

수율 100.1%

3-(undecanyloxy)benzoyl chloride

수율 100.1%

용매

DCM

반응 조건

후처리

1. 1
   농축concentrated

실험 절차

1 mL of oxalyl chloride (11.5 mmol) and two drops of anhydrous DMF are added under argon to 93 mg of toluene-dried acid 22 (318 μmol) dissolved in 20 mL of anhydrous DCM. The medium is stirred at room temperature for two hours, and then concentrated to give 99 mg of a yellow oil, i.e. a yield of 99%.

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