반응 #417904
ord-9eb251ab9d2f4dd397596f5f2a9d6088
반응 방정식
Desmorapid
n-hexyl isocyanate
isocyanate
→
Isopropyl hexylcarbamate
반응 조건
온도
60°CELSIUS
상세 조건
See reaction.notes.procedure_details.
후처리
- 1온도Thereafter, cooling
- 2기타the product was obtained as a clear liquid
실험 절차
In a 250 ml round-bottomed flask, 0.02 g of Desmorapid Z, 34.0 g of n-hexyl isocyanate were initially introduced and heated to 60° C. Thereafter, 16.0 g of isopropanol were added dropwise and the mixture was further kept at 60° C. until the isocyanate content had fallen below 0.1%. Thereafter, cooling was effected and the product was obtained as a clear liquid.