반응 #41778

ord-423ac40369184f8fa67c4d931eed13e0

용매

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    여과The catalyst was filtered off
  2. 2
    농축the solvent was concentrated

실험 절차

A solution of {4-[2-methoxy-4-(methylamino)-5-nitrophenoxy](2-pyridyl)}-N-methylcarboxamide. In methanol was hydrogenated with 10% Pd/C. The catalyst was filtered off and the solvent was concentrated to yield {4-[3-amino-6-methoxy-4-(methylamino)phenoxy](2-pyridyl)}-N-methylcarboxamide. MS: MH+: 302.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07728010B2uspto-grants-2010_06