반응 #417011
ord-f1dfed6d36574850a6245e0f377c767f
용매
반응 조건
상세 조건
See reaction.notes.procedure_details.
실험 절차
By following the same procedure as the 2nd step of Example 12 except that 10.0 g of 1-methylphenylphosphanium carbonate, 6.9 g of 60% perchlorate, and 10.0 g of water were used, 10.9 g (94.8% of the theoretical yield, yield of 67.6% to 1-phenylphosphane) of methylphosphanium perchlorate was obtained.