반응 #414645

반응 방정식

6-bromo-1,2,3,4-tetrahydro-8-nitro-N,N-dipropyl-3-quinolinamine

→

1,2,3,4-tetrahydro-N3,N3 -dipropyl-3,8-quinolinediamine

수율 101.3%

용매

ethanol

반응 조건

후처리

1. 1
   여과The solution was filtered
2. 2
   기타the ethanol evaporated

실험 절차

A mixture of 6-bromo-1,2,3,4-tetrahydro-8-nitro-N,N-dipropyl-3-quinolinamine (2.7 g) and 10% palladium charcoal (0.5 g) in ethanol (150 mL) was hydrogenated for 18 hours. The solution was filtered and the ethanol evaporated to give 1.9 g of 1,2,3,4-tetrahydro-N3,N3 -dipropyl-3,8-quinolinediamine as an oil.

출처