반응 #414464

반응 방정식

1,3-dimethyl-3-(2-ethylhexanoylperoxy)butyl chloroformate

hydrazine

phosgene

1,3-Dimethyl-3-(2-ethylhexanoylperoxy)butyl chloroformate

→

1,3-Dimethyl-3-(2-ethylhexanoylperoxy)butyl carbazate

반응 조건

후처리

1. 1
   기타followed by removal of excess phosgene

실험 절차

1,3-Dimethyl-3-(2-ethylhexanoylperoxy)butyl carbazate was prepared by reacting 1,3-dimethyl-3-(2-ethylhexanoylperoxy)butyl chloroformate with 11 molar excess of 54% aqueous hydrazine. 1,3-Dimethyl-3-(2-ethylhexanoylperoxy)butyl chloroformate was initially prepared with a purity of 72% by reacting 3-hydroxy-1,1-dimethylbutyl peroxy-2-ethylhexanoate with excess phosgene followed by removal of excess phosgene.

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