반응 #413613

반응 방정식

Zirconium oxychloride

disodium hydrogenphosphate

→

zirconium phosphate

수율 123.4%

용매

water

반응 조건

후처리

1. 1
   기타to form a white precipitate
2. 2
   세척the white precipitate was sufficiently washed with water by a decantation method
3. 3
   여과filtered
4. 4
   세척further washed with water
5. 5
   기타dried at 120° C.

실험 절차

Zirconium oxychloride (ZrOCl2.8H2O) 36.1 g (0.112 mole) was dissolved in 50 ml of water, and to the resulting solution was added 200 ml of an aqueous solution containing disodium hydrogenphosphate (Na2HPO4) 31.8 g (0.224 mole) to form a white precipitate. The resulting mixture was stirred at 80° C. for one hour, and the white precipitate was sufficiently washed with water by a decantation method, filtered, further washed with water, and dried at 120° C. to obtain zirconium phosphate (Zr(HPO4)2) 30.1 g.

출처