반응 #41306

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(S)-tert-butyl 1-(methoxy(methyl)amino)-1-oxopropan-2-ylcarbamate

(3-ethylphenyl)magnesium bromide

THF

→

subtitle compound

(S)-tert-butyl 1-(3-ethylphenyl)-1-oxopropan-2-ylcarbamate

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실험 절차

The subtitle compound was prepared analogous to the method described in Example 19 (step 19d). Starting from (S)-tert-butyl 1-(methoxy(methyl)amino)-1-oxopropan-2-ylcarbamate (0.7 g, 3.01 mmol) and freshly made (3-ethylphenyl)magnesium bromide 0.9M solution in THF (5 mL, 4.50 mmol). Yield 817 mg (97%)

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