반응 #412766

반응 방정식

p-Dioxanone

3-methyl-2,5- morpholinedione

1-dodecanol

stannous octoate

→

p-Dioxanone 3-Methyl-2,5-Morpholinedione

용매

toluene

반응 조건

후처리

1. 1
   workup.ADDITIONmagnetically mixed in
2. 2
   온도a flame
3. 3
   기타vacuum dried
4. 4
   기타sealed glass ampoule

실험 절차

p-Dioxanone (12.8 g, 0.125 moles), 3-methyl-2,5- morpholinedione (0.5 g, 0.00388 moles), 1-dodecanol (0.0369 g, 0.000198 moles), and a catalytic amount of stannous octoate (0.025 ml of a 0.33 M toluene solution, 0.0000083 moles) are heated and magnetically mixed in a flame and vacuum dried, sealed glass ampoule according to the following temperature/time scheme:

출처