반응 #412762

반응 방정식

p-Dioxanone

2,5-morpholinedione

1-dodecanol

stannous octoate

→

3 -p-Dioxanone 2,5-Morpholinedione

용매

toluene

반응 조건

후처리

1. 1
   workup.ADDITIONmagnetically mixed in
2. 2
   온도a flame
3. 3
   기타vacuum dried
4. 4
   기타sealed glass ampoule

실험 절차

p-Dioxanone (20.1 g, 0.197 moles), 2,5-morpholinedione (0.7 g, 0.00609 moles), 1-dodecanol (0.0623 g, 0.000334 moles), and a catalytic amount of stannous octoate (0.51 ml of a 0.0264 M toluene solution, 0.0000135 moles) are heated and magnetically mixed in a flame and vacuum dried, sealed glass ampoule according to the following temperature/time scheme:

출처