반응 #411324

ord-4ec6c7557f71461d85c514093cfbb975

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타to dry at ambient temperature for approximately 20 minutes
  2. 2
    온도The painted titanium substrate was subsequently heat
  3. 3
    workup.ADDITIONtreated in a furnace
  4. 4
    기타at approximately 500° C.
  5. 5
    기타for approximately 20-30 minutes

실험 절차

After the titanium substrate surface was roughened, it was painted with a n-butanol solution containing salts of iridium and tantalum in a ratio of iridium to tantalum of approximately 65% to 35% by weight. The applied solution was allowed to dry at ambient temperature for approximately 20 minutes. The painted titanium substrate was subsequently heat treated in a furnace having an oxygen containing atmosphere at approximately 500° C. for approximately 20-30 minutes to form an iridium oxide/tantalum oxide composite coating. The process of painting and heat treating the titanium substrate was repeated in order to obtain a total loading of about 2.0 g/m2. After this loading was achieved, the painted substrate was heat treated for approximately one hour at approximately 500° C.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US06217729B1uspto-grants-2001_04