반응 #409753
ord-231981908a694978b11ad2fdec7dfee1
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타on a rotary evaporator under reduced pressure
- 2기타The residue obtained in this way
- 3기타is recrystallized from water
실험 절차
Cyanoacetyldimethylurea is prepared in analogy to Example 1. Instead of dibenzylurea, dimethylurea is employed. The product is worked up by stripping off the acetic anhydride/acetic acid mixture on a rotary evaporator under reduced pressure. The residue obtained in this way is recrystallized from water.