반응 #409537

ord-b204d3d6fd5b41618b36b5b1fc2e0611

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

In substantially the same manner as in Working Example 8, imidazole was allowed to react with 6-[4-[2-[(E) -2-phenylethenyl]-4-oxazolylmethoxy]phenyl]hexyl methanesulfonate to give 4-[4-[6-(1-imidazolyl)hexyl]phenoxymethyl]-2-[(E)-2-phenylethenyl]oxazole. The yield was 66%. Recrystallization from ethyl acetate-hexane gave colorless prisms, mp 108-109° C.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US06211215B1uspto-grants-2001_04